Free Standard AU & NZ Shipping For All Book Orders Over $80!
Register      Login
Australian Journal of Chemistry Australian Journal of Chemistry Society
An international journal for chemical science
Shopping Cart: ( empty )
You are here: Home > Journals > CH > CH16322
RESEARCH ARTICLE
Contents Vol 70(1)

Optimised Syntheses of the Half-Sandwich Complexes FeCl(dppe)Cp*, FeCl(dppe)Cp, RuCl(dppe)Cp*, and RuCl(dppe)Cp

Josef B. G. Gluyas A , Neil J. Brown B , Julian D. Farmer B and Paul J. Low A C
+ Author Affiliations
- Author Affiliations

A School of Chemistry and Biochemistry, University of Western Australia, 35 Stirling Highway, Crawley, WA 6009, Australia.

B Department of Chemistry, Durham University, South Road, Durham DH1 3LE, UK.

C Corresponding author. Email: paul.low@uwa.edu.au

Australian Journal of Chemistry 70(1) 113-119 https://doi.org/10.1071/CH16322
Submitted: 25 May 2016  Accepted: 19 June 2016   Published: 28 July 2016

Abstract

Thanks to their synthetic versatility, the half-sandwich metal chlorides MCl(dppe)(η5-C5R5) [M = Fe, Ru; dppe = 1,2-bis(diphenylphosphino)ethane, R = H (cyclopentadiene, Cp), CH3 (pentamethylcyclopentadiene, Cp*)] are staple starting materials in many organometallic laboratories. Here we present an overview of the synthetic methods currently available for FeCl(dppe)Cp*, FeCl(dppe)Cp, RuCl(dppe)Cp*, and RuCl(dppe)Cp, and describe in detail updated and optimised multigram syntheses of all four compounds.


References

[1]  R. Poli, Chem. Rev. 1991, 91, 509.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaK3MXktVyrtr8%3D&md5=275562309903742b84f218718ef88110CAS |

[2]  N. J. Coville, K. E. du Plooy, W. Pickl, Coord. Chem. Rev. 1992, 116, 1.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaK38XlsFWjtr4%3D&md5=dd29277adaf54a1b6d6832d1cbb223d2CAS |

[3]  V. C. Gibson, S. K. Spitzmesser, Chem. Rev. 2003, 103, 283.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BD38XpsFCmsrc%3D&md5=ee69601b6f4acf5c5cdbdbe5ed729e3cCAS | 12517186PubMed |

[4]  K. C. Hultzsch, P. Voth, K. Beckerle, T. P. Spaniol, J. Okuda, Organometallics 2000, 19, 228.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BD3cXmtVWqtw%3D%3D&md5=17fd746f6a99d5de353ad1c3990b1395CAS |

[5]  E. Le Grognec, J. Claverie, R. Poli, J. Am. Chem. Soc. 2001, 123, 9513.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BD3MXms1amsLw%3D&md5=731f1862cbcd57528246edaa342c24d4CAS | 11572671PubMed |

[6]  D. J. Jones, V. C. Gibson, S. M. Green, P. J. Maddox, A. J. P. White, D. J. Williams, J. Am. Chem. Soc. 2005, 127, 11037.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BD2MXmt1WktLg%3D&md5=b75c0c97bde3a3b4e1b115b0219a4b81CAS | 16076211PubMed |

[7]  C. Ganter, Chem. Soc. Rev. 2003, 32, 130.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BD3sXjtFGmt7s%3D&md5=322853b2455af03421fbba8e946f3c99CAS | 12792936PubMed |

[8]  R. L. Halterman, Chem. Rev. 1992, 92, 965.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaK38XkvFSgtrw%3D&md5=c356286615c5c15fc76a9feb9b4530e7CAS |

[9]  G. Consiglio, F. Morandini, Chem. Rev. 1987, 87, 761.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaL2sXksF2jtL0%3D&md5=7e695a94414594479d44a01231f574a8CAS |

[10]  C. G. Newton, D. Kossler, N. Cramer, J. Am. Chem. Soc. 2016, 138, 3935.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BC28XisVWmt7s%3D&md5=7b8ab1a1bd7d31c5a06f09891ab5d9cbCAS |

[11]  U. Siemeling, Chem. Rev. 2000, 100, 1495.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BD3cXhvVyktLk%3D&md5=dda9d5f6f12d6bc8eefd8c3a9f857ddeCAS | 11749274PubMed |

[12]  E. B. Bauer, Chem. Soc. Rev. 2012, 41, 3153.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BC38XksVOhu7k%3D&md5=ee1e7e82c9ad808ec00a0ed656e07e2fCAS | 22306968PubMed |

[13]  C. G. Hartinger, P. J. Dyson, Chem. Soc. Rev. 2009, 38, 391.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BD1MXksVSntLs%3D&md5=d5056cd8273e3d9a0bda4c3024312f46CAS | 19169456PubMed |

[14]  E. Meggers, Curr. Opin. Chem. Biol. 2007, 11, 287.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BD2sXmvVOnsr8%3D&md5=33f7594c0553574d4e566e7ebde5313bCAS | 17548234PubMed |

[15]  K. J. Kilpin, P. J. Dyson, Chem. Sci. 2013, 4, 1410.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BC3sXjtlyms7c%3D&md5=7bf5654d8e43b6be28eed982411852d9CAS |

[16]  G. Süss-Fink, Dalton Trans. 2010, 39, 1673.
         | Crossref | GoogleScholarGoogle Scholar | 20449402PubMed |

[17]  H. Werner, Organometallics 2005, 24, 1036.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BD2MXhtFensrk%3D&md5=76c0ad9a7959296494020325c5918bfeCAS |

[18]  J. M. Lynam, Chem. – Eur. J. 2010, 16, 8238.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BC3cXptlejtL8%3D&md5=3a5488f688eb5b782a55883a6a985b27CAS | 20607768PubMed |

[19]  P. B. Glaser, T. D. Tilley, Organometallics 2004, 23, 5799.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BD2cXptValtL4%3D&md5=e01f27cccf45e03c13292576b5ff868eCAS |

[20]  P. J. Low, M. I. Bruce, Adv. Organomet. Chem. 2001, 48, 71.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BD38XnsVSjsg%3D%3D&md5=c03cb957b4aadb5f768320e883b28af9CAS |

[21]  M. I. Bruce, P. J. Low, Adv. Organomet. Chem. 2004, 50, 179.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BD2cXktlansb8%3D&md5=d643a3e3303676c87a741d0ba2a3e60eCAS |

[22]  Y.-F. Han, W.-G. Jia, W.-B. Yu, G.-X. Jin, Chem. Soc. Rev. 2009, 38, 3419.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BD1MXhsVanurrE&md5=411b3b9600d67f8ad3ee3b44826c9338CAS | 20449060PubMed |

[23]  G.-L. Wang, Y.-J. Lin, H. Berke, G.-X. Jin, Inorg. Chem. 2010, 49, 2193.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BC3cXhtlWlu7o%3D&md5=f9146192c85ef9ed32982b22c4bc367bCAS | 20121071PubMed |

[24]  B. Therrien, Eur. J. Inorg. Chem. 2009, 2009, 2445.
         | Crossref | GoogleScholarGoogle Scholar |

[25]  J. Mattsson, P. Govindaswamy, A. K. Renfrew, P. J. Dyson, P. Štěpnička, G. Süss-Fink, B. Therrien, Organometallics 2009, 28, 4350.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BD1MXnsVeiurg%3D&md5=af51dcf4b08accb6f2055f3a436c2a36CAS |

[26]  N. Gauthier, G. Argouarch, F. Paul, M. G. Humphrey, L. Toupet, S. Ababou-Girard, H. Sabbah, P. Hapiot, B. Fabre, Adv. Mater. 2008, 20, 1952.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BD1cXns1ymtL8%3D&md5=f3618679656e5ba0e222ad84c8e0b401CAS |

[27]  G. Grelaud, N. Gauthier, Y. Luo, F. Paul, B. Fabre, F. Barrière, S. Ababou-Girard, T. Roisnel, M. G. Humphrey, J. Phys. Chem. C 2014, 118, 3680.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BC2cXht12mu70%3D&md5=81ed23eab6efb652c9ebfc9fbe469690CAS |

[28]  M. H. Garcia, M. P. Robalo, A. R. Dias, M. T. Duarte, W. Wenseleers, G. Aerts, E. Goovaerts, M. P. Cifuentes, S. Hurst, M. G. Humphrey, M. Samoc, B. Luther-Davies, Organometallics 2002, 21, 2107.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BD38XivVGnt78%3D&md5=d24f18591d454ecd846dcc540788b991CAS |

[29]  Q. Ge, G. T. Dalton, M. G. Humphrey, M. Samoc, T. S. A. Hor, Chem. Asian J. 2009, 4, 998.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BD1MXnsF2kur0%3D&md5=651bd0da181b817760d7ac7c790600b0CAS | 19434645PubMed |

[30]  Q. Ge, T. C. Corkery, M. G. Humphrey, M. Samoc, T. S. A. Hor, Dalton Trans. 2009, 6192.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BD1MXptVKksbs%3D&md5=4f48a264c23eaa4ca14ddce8f94a55e5CAS | 20449116PubMed |

[31]  M. P. Cifuentes, M. G. Humphrey, J. P. Morrall, M. Samoc, F. Paul, C. Lapinte, T. Roisnel, Organometallics 2005, 24, 4280.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BD2MXmtVChtb4%3D&md5=3e1b7233df0676bfd095a9cec886972dCAS |

[32]  N. Gauthier, G. Argouarch, F. Paul, L. Toupet, A. Ladjarafi, K. Costuas, J.-F. Halet, M. Samoc, M. P. Cifuentes, T. C. Corkery, M. G. Humphrey, Chem. – Eur. J. 2011, 17, 5561.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BC3MXls1CmsL4%3D&md5=cf7f8621dba0e9801d1c81aba5387390CAS | 21495098PubMed |

[33]  F. Malvolti, C. Rouxel, A. Triadon, G. Grelaud, N. Richy, O. Mongin, M. Blanchard-Desce, L. Toupet, F. I. A. Razak, R. Stranger, M. Samoc, X. Yang, G. Wang, A. Barlow, M. P. Cifuentes, M. G. Humphrey, F. Paul, Organometallics 2015, 34, 5418.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BC2MXhvVentrfO&md5=a87372d759d077834ed341a131247d7eCAS |

[34]  W. E. Geiger, F. Barrière, Acc. Chem. Res. 2010, 43, 1030.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BC3cXjvFCjsbs%3D&md5=0509cf41f8e78b15772d5aa60265f5ecCAS | 20345126PubMed |

[35]  W. E. Geiger, Coord. Chem. Rev. 2013, 257, 1459.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BC38XhtFahtLnO&md5=078fe0ac690464870160558d47d97305CAS |

[36]  M. Parthey, J. B. G. Gluyas, M. A. Fox, P. J. Low, M. Kaupp, Chem. – Eur. J. 2014, 20, 6895.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BC2cXmsVWmsbY%3D&md5=61db98fa26fe467b5d09f32e2fa790c9CAS | 24740610PubMed |

[37]  P. J. Low, Coord. Chem. Rev. 2013, 257, 1507.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BC38Xhtl2gtb3I&md5=5b8468d7f23fa68c20a25bf0dee3b874CAS |

[38]  J.-F. Halet, C. Lapinte, Coord. Chem. Rev. 2013, 257, 1584.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BC38XhsFalsLbL&md5=1fe51b79185676db1f104426630e4882CAS |

[39]  R. Dembinski, T. Bartik, B. Bartik, M. Jaeger, J. A. Gladysz, J. Am. Chem. Soc. 2000, 122, 810.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BD3cXltVyhsw%3D%3D&md5=0f3ce73f31e25b0146a19becc6a1bfbdCAS |

[40]  K. Venkatesan, O. Blacque, H. Berke, Dalton Trans. 2007, 1091.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BD2sXisVKksL8%3D&md5=99f9b017aee5b4ade7d4bab9382c3255CAS | 17339991PubMed |

[41]  M. J. Mays, P. L. Sears, J. Chem. Soc., Dalton Trans. 1973, 1873.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaE2cXjs1Sl&md5=67d5082106071d9877d2ea4a8245d9beCAS |

[42]  G. S. Ashby, M. I. Bruce, I. B. Tomkins, R. C. Wallis, Aust. J. Chem. 1979, 32, 1003.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaE1MXlvFegu7c%3D&md5=337f7bcb4d0818ebb21ee89cc5abd4f7CAS |

[43]  Y. Mutoh, Y. Ikeda, Y. Kimura, Y. Ishii, Chem. Lett. 2009, 38, 534.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BD1MXnvFGksbg%3D&md5=3fbee6d4ae7444b52a40a2e45c37cbe0CAS |

[44]  E. M. Long, N. J. Brown, W. Y. Man, M. A. Fox, D. S. Yufit, J. A. K. Howard, P. J. Low, Inorg. Chim. Acta 2012, 380, 358.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BC38XhtFShs7Y%3D&md5=2651572d559c064edb9bccf7956cd642CAS |

[45]  C.-W. Chang, P.-C. Ting, Y.-C. Lin, G.-H. Lee, Y. Wang, J. Organomet. Chem. 1998, 553, 417.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaK1cXisVCktro%3D&md5=4d669df078e51c3b7522b144d3c2dd53CAS |

[46]  A. P. Shaw, B. L. Ryland, J. R. Norton, D. Buccella, A. Moscatelli, Inorg. Chem. 2007, 46, 5805.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BD2sXmsVaju70%3D&md5=04bd9ae57907b00ea3260cc14cdf3536CAS | 17569530PubMed |

[47]  A. Burgun, F. Gendron, P. A. Schauer, B. W. Skelton, P. J. Low, K. Costuas, J.-F. Halet, M. I. Bruce, C. Lapinte, Organometallics 2013, 32, 5015.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BC3sXosVaqur8%3D&md5=157a016f618f7683c95d4fd237ab5d9eCAS |

[48]  C. Roger, P. Marseille, C. Salus, J. R. Hamon, C. Lapinte, J. Organomet. Chem. 1987, 336, C13.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaL1cXmtlWhsL0%3D&md5=379ad07baa9ccabda30fcf73c0e79cdbCAS |

[49]  C. Roger, P. Hamon, L. Toupet, H. Rabaa, J. Y. Saillard, J.-R. Hamon, C. Lapinte, Organometallics 1991, 10, 1045.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaK3MXhs1Cntrg%3D&md5=515e4993f5946a2d35a7d410c64ea563CAS |

[50]  H. Lehmkuhl, G. Mehler, R. Benn, A. Rufińska, G. Schroth, C. Krüger, E. Raabe, Chem. Ber. 1987, 120, 1987.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaL1cXit1Shtg%3D%3D&md5=81923efd033f9aec0cfd754cd6796863CAS |

[51]  D. Patel, A. Wooles, A. D. Cornish, L. Steven, E. S. Davies, D. J. Evans, J. McMaster, W. Lewis, A. J. Blake, S. T. Liddle, Dalton Trans. 2015, 44, 14159.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BC2MXhtFyqtL3M&md5=adbb6cbff926051ae9aee096c0ed6e82CAS | 26185807PubMed |

[52]  D. W. Macomber, M. D. Rausch, J. Am. Chem. Soc. 1983, 105, 5325.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaL3sXkslSru7w%3D&md5=b26c8890fd3ef99db4284a407fde054aCAS |

[53]  U. Behrens, R. E. Dinnebier, S. Neander, F. Olbrich, Organometallics 2008, 27, 5398.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BD1cXhtFWmt7rF&md5=5ed17c11ebc3b63239384ed5bb690868CAS |

[54]  R. Langer, F. Bönisch, L. Maser, C. Pietzonka, L. Vondung, T. P. Zimmermann, Eur. J. Inorg. Chem. 2015, 2015, 141.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BC2cXhvF2kt77F&md5=bf83a58bded21956cace15add00208e9CAS |

[55]  T. S. Piper, F. A. Cotton, G. Wilkinson, J. Inorg. Nucl. Chem. 1955, 1, 165.
         | Crossref | GoogleScholarGoogle Scholar |

[56]  E. O. Fischer, E. Moser, Inorg. Synth. 1970, 12, 35.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaE3MXhtlamsw%3D%3D&md5=d44a4665f2bd57ccc02146534e4fe78fCAS |

[57]  R. B. King, L. W. Houk, K. H. Pannell, Inorg. Chem. 1969, 8, 1042.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaF1MXktVensb8%3D&md5=328fbe2742be18cb1088bd421f4cf8d4CAS |

[58]  D. Astruc, Tetrahedron 1983, 39, 4027.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaL2cXhtl2itLg%3D&md5=186456b855f99fa77d11cb22af4a29bbCAS |

[59]  J. Ruiz, M. Lacoste, D. Astruc, J. Am. Chem. Soc. 1990, 112, 5471.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaK3cXltFGnu7w%3D&md5=5a90e9ccaef2dc9dc4a10db0fc9dfab0CAS |

[60]  D. H. Hill, M. A. Parvez, A. Sen, J. Am. Chem. Soc. 1994, 116, 2889.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaK2cXitFyjtbs%3D&md5=21f9588bbb132840cd9661d7ed9f3782CAS |

[61]  J. A. van Rijn, E. Gouré, M. A. Siegler, A. L. Spek, E. Drent, E. Bouwman, J. Organomet. Chem. 2011, 696, 1899.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BC3MXltFKhtrk%3D&md5=0bd133c62f115e4f2807b34d25de97bfCAS |

[62]  S. El-Tarhuni, M. Ho, M. H. Kawser, S. Shi, M. W. Whiteley, J. Organomet. Chem. 2014, 752, 30.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BC2cXltVaisg%3D%3D&md5=bc7584d759e08bb7610180b999da70e3CAS |

[63]  K. Ziegler, H. Froitzheim-Kühlhorn, K. Hafner, Chem. Ber. 1956, 89, 434.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaG28XnslKjsQ%3D%3D&md5=244329ce053384e4ee6694c159e97d60CAS |

[64]  J. Thiele, Chem. Ber. 1901, 34, 68.
         | Crossref | GoogleScholarGoogle Scholar |

[65]  O. T. Beachley, J. C. Pazik, T. E. Glassman, M. R. Churchill, J. C. Fettinger, R. Blom, Organometallics 1988, 7, 1051.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaL1cXitVCltb8%3D&md5=b304375cb51993466eb6ecd94c0f9dd3CAS |

[66]  P. M. Treichel, D. A. Komar, P. J. Vincenti, Synth. React. Inorg. Met.-Org. Chem. 1984, 14, 383.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaL2cXlslWntb8%3D&md5=978d35b21d2d18b2eab961a3a01c11fdCAS |

[67]  M. I. Bruce, C. Hammeister, A. G. Swincer, R. C. Wallis, Inorg. Synth. 1982, 21, 78.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaL3sXnt1ekuw%3D%3D&md5=628303716e08f01cc777c7cfd08389acCAS |

[68]  T. D. Tilley, R. H. Grubbs, J. E. Bercaw, Organometallics 1984, 3, 274.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaL2cXmvVCqsg%3D%3D&md5=33932a1a4e60917bfd1b63f2d9b24fc0CAS |

[69]  N. Oshima, H. Suzuki, Y. Moro-Oka, Chem. Lett. 1984, 7, 1161.
         | Crossref | GoogleScholarGoogle Scholar |

[70]  U. Koelle, J. Kossakowski, J. Organomet. Chem. 1989, 362, 383.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaL1MXmtFCltbw%3D&md5=3bcdae59b70237196899ea48e7d55c8fCAS |

[71]  L. Luo, N. Zhu, N.-J. Zhu, E. D. Stevens, S. P. Nolan, Organometallics 1994, 13, 669.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaK2cXislSksbc%3D&md5=a9b56c72df9666163ce74bfe8b7aba89CAS |

[72]  D.-H. Lee, J. Korean Chem. Soc. 1992, 36, 248.
         | 1:CAS:528:DyaK38XksVyrt7o%3D&md5=0975e9fbee1167fe827abe7d73c2922fCAS |

[73]  M. I. Bruce, B. G. Ellis, P. J. Low, B. W. Skelton, A. H. White, Organometallics 2003, 22, 3184.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BD3sXltFCiu70%3D&md5=7b2cfbe6ad760278518952a12aedd8ccCAS |

[74]  K. S. Singh, C. Thöne, M. R. Kollipara, J. Organomet. Chem. 2005, 690, 4222.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BD2MXpt1ehurk%3D&md5=c943d6abbe5c1bac14794667f74048fbCAS |

[75]  S. G. Davies, F. Scott, J. Organomet. Chem. 1980, 188, C41.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaL3cXkslWqsbc%3D&md5=6d4c1986a732eff5b751c70cc4eb8589CAS |

[76]  P. M. Treichel, D. A. Komar, Synth. React. Inorg. Met.-Org. Chem. 1980, 10, 205.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaL3cXls1ygur0%3D&md5=118c8f1d0ba55d1b9c9740641d26aff1CAS |

[77]  G. Consiglio, F. Morandini, F. Bangerter, Inorg. Chem. 1982, 21, 455.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaL38XjsFGjtA%3D%3D&md5=94228860d7ebb23a1e287df4b334d1d8CAS |

[78]  A. Gutierrez Alonso, L. Ballester Reventos, J. Organomet. Chem. 1988, 338, 249.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaL1MXjvFWntw%3D%3D&md5=9f0d50f240d4fcaae00ed2c9c19f0f47CAS |

[79]  L. Ballester, A. Gutierrez, M. F. Perpinan, J. Chem. Educ. 1989, 66, 777.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaK3cXmslCm&md5=b4f19cf674b6ff2d2499abc6abda45baCAS |

[80]  E. M. Moura, M. H. Dickman, H. G. L. Siebald, G. J. Gama, Polyhedron 1999, 18, 2899.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaK1MXnt1Whs7k%3D&md5=e19f17941e21ceec67e1241d0d336738CAS |

[81]  M. I. Bruce, M. G. Humphrey, J. M. Patrick, A. H. White, Aust. J. Chem. 1983, 36, 2065.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaL2cXktVOgur8%3D&md5=dcefccbf22a83678a0fb8f2152016350CAS |

[82]  H. Nagashima, K. Yamaguchi, K. Mukai, K. Itoh, J. Organomet. Chem. 1985, 291, c20.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaL28Xit1Gjs78%3D&md5=fda8440cfc3ddfaf64d407f160f195b5CAS |

[83]  M. O. Albers, H. E. Oosthuizen, D. J. Robinson, A. Shaver, E. Singleton, J. Organomet. Chem. 1985, 282, c49.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaL2MXltVGisb8%3D&md5=bfb31facff9a08091a5f2914084ffb2aCAS |

[84]  M. O. Albers, D. J. Robinson, A. Shaver, E. Singleton, Organometallics 1986, 5, 2199.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaL28XmtV2itb4%3D&md5=d70970a821f58303fb074b2608a18af2CAS |

[85]  D. S. Perekalin, E. E. Karslyan, E. A. Trifonova, A. I. Konovalov, N. L. Loskutova, Y. V. Nelyubina, A. R. Kudinov, Eur. J. Inorg. Chem. 2013, 2013, 481.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BC38XhslOrsrvL&md5=e2c24e79b2bb4d610c69768e525c67dcCAS |

[86]  D. E. Bublitz, W. E. McEwen, J. Kleinberg, Org. Synth. 1961, 41, 96.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaF38XksFClsQ%3D%3D&md5=5e7afb2871e57f0f81ffdef224868d8cCAS |

[87]  D. S. Perekalin, E. E. Karslyan, P. V. Petrovskii, A. O. Borissova, K. A. Lyssenko, A. R. Kudinov, Eur. J. Inorg. Chem. 2012, 2012, 1485.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BC3MXhsV2ru7%2FN&md5=c1d29693ad96597e7c1170f97f394f53CAS |

[88]  J. Chatt, R. G. Hayter, J. Chem. Soc. (Res) 1961, 896.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaF3MXos1amsw%3D%3D&md5=ba82f63f80c90bd6fdcac2b8c2cbb848CAS |

[89]  E. M. Moura, M. H. Dickman, H. G. L. Siebald, G. J. Gama, Polyhedron 1999, 18, 2899.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaK1MXnt1Whs7k%3D&md5=e19f17941e21ceec67e1241d0d336738CAS |

[90]  R. S. Dickson, B. J. Dobney, F. W. Eastwood, J. Chem. Educ. 1987, 64, 898.
         | Crossref | GoogleScholarGoogle Scholar |

[91]  G. R. Fulmer, A. J. M. Miller, N. H. Sherden, H. E. Gottlieb, A. Nudelman, B. M. Stoltz, J. E. Bercaw, K. I. Goldberg, Organometallics 2010, 29, 2176.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DC%2BC3cXkslKms7Y%3D&md5=4355b5cc11d90e309f18cd3d9c6917c2CAS |

[92]  U. Edlund, Org. Magn. Reson. 1977, 9, 593.
         | Crossref | GoogleScholarGoogle Scholar | 1:CAS:528:DyaE1cXhs12iu7o%3D&md5=753e5b20a649df4800f67e09173dbad6CAS |