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RESEARCH ARTICLE
Contents Vol 70(1)

Optimised Syntheses of the Half-Sandwich Complexes FeCl(dppe)Cp*, FeCl(dppe)Cp, RuCl(dppe)Cp*, and RuCl(dppe)Cp

Josef B. G. Gluyas A , Neil J. Brown B , Julian D. Farmer B and Paul J. Low A C
+ Author Affiliations
- Author Affiliations

A School of Chemistry and Biochemistry, University of Western Australia, 35 Stirling Highway, Crawley, WA 6009, Australia.

B Department of Chemistry, Durham University, South Road, Durham DH1 3LE, UK.

C Corresponding author. Email: paul.low@uwa.edu.au

Australian Journal of Chemistry 70(1) 113-119 https://doi.org/10.1071/CH16322
Submitted: 25 May 2016  Accepted: 19 June 2016   Published: 28 July 2016

Abstract

Thanks to their synthetic versatility, the half-sandwich metal chlorides MCl(dppe)(η5-C5R5) [M = Fe, Ru; dppe = 1,2-bis(diphenylphosphino)ethane, R = H (cyclopentadiene, Cp), CH3 (pentamethylcyclopentadiene, Cp*)] are staple starting materials in many organometallic laboratories. Here we present an overview of the synthetic methods currently available for FeCl(dppe)Cp*, FeCl(dppe)Cp, RuCl(dppe)Cp*, and RuCl(dppe)Cp, and describe in detail updated and optimised multigram syntheses of all four compounds.


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