Free Standard AU & NZ Shipping For All Book Orders Over $80!
Register      Login
Australian Energy Producers Journal Australian Energy Producers Journal Society
Journal of Australian Energy Producers
RESEARCH ARTICLE

A Mesoproterozoic (~1.25 Ga) ‘fossilised’ oil column in the Moroak Sandstone of the Beetaloo Sub-basin, NT

Richard Kempton https://orcid.org/0000-0003-3107-5526 A * , Siyumini Perera A , Mohinudeen Faiz B and Michael Verrall A
+ Author Affiliations
- Author Affiliations

A CSIRO, Kensington, WA, Australia.

B CSIRO, Pullenvale, Qld, Australia.




Richard Kempton holds a BSc (Hons) in Geology from the University of Melbourne and a PhD from the University of Western Australia. Richard is a Senior Research Scientist with the Geofluids Team at CSIRO Energy in Perth and is a domain expert in fluid inclusions with 20+ years’ experience in reconstructing charge histories for petroleum systems analysis. More recently, he has been working on CO2 and hydrogen-related projects and geological applications of machine learning. Prior to joining CSIRO, Richard worked for the Queensland Gas Company. He is a member of PESA and the Geological Society of Australia.



Siyumini Perera recently obtained her PhD from the University of Queensland, where she focussed on Early Paleozoic biostratigraphy and imaging of microfossils using micro-computed tomography. Since early 2023, she has joined the Geofluids Team at CSIRO Energy in Perth as a Research Technician and conducts various analyses to quantify and characterise geofluids within sedimentary basins and basement.



Mohinudeen Faiz is a Geoscientist with 30+ years’ experience in petroleum exploration, development and research activities. Faiz holds PhD and MSc degrees from the University of Wollongong (Australia) and a BSc (Hons) degree from the University of Peradeniya (Sri Lanka). He is currently a Principal Research Scientist at CSIRO Energy where he focuses on basin modelling for petroleum systems and low-emission natural energy sources. Previously, Faiz worked at Origin Energy where he was an organic geochemistry and petroleum systems modelling subject matter expert and contributed to both conventional and unconventional exploration and production projects in various basins in Australia and overseas. He is a member of the American Association of Petroleum Geologists, PESA and International Committee for Coal and Organic Petrology.



Michael Verrall is a Senior Research Scientist at CSIRO and is the Manager of the Electron Beam and X-ray Laboratories at the Australian Resource Research Centre. His interests are in scientific instrumentation and developing scanning electron microscopy and X-ray based techniques for automated mineralogy. Michael has a BSc degree in physics and previous experience working in the mining industry and also works as a Radiation Safety Officer for CSIRO.

* Correspondence to: Richard.Kempton@csiro.au

Australian Energy Producers Journal 64 169-185 https://doi.org/10.1071/EP23047
Submitted: 15 December 2023  Accepted: 1 February 2024  Published: 16 May 2024

© 2024 The Author(s) (or their employer(s)). Published by CSIRO Publishing on behalf of Australian Energy Producers.

Abstract

The Beetaloo Sub-basin hosts a large unconventional ‘shale gas’ resource within organic-rich Mesoproterozoic shales of the Velkerri and Kyalla formations; however, little has been done to understand conventional oil charge to the associated sandstone reservoirs. Using Grains containing Oil Inclusions, we show that an ancient ‘fossilised’ oil column once existed at the top of the Moroak Sandstone in the Elliott-1 well. The column had a minimum height of 18.02 m, with a possible paleo–oil–water contact at the base of a resistive zone on logs at ~1348 m and a change in core colour. Fluid inclusion oil is entrapped in quartz cement and is inferred to be a light oil of >42°API gravity from its near-blue fluorescence colour. Post-oil solid bitumen is still present in the reservoir sandstone, and we assert that this helped to retard the crystallisation of quartz cement that elsewhere occluded porosity. From burial history models that utilise a refined source rock maturity evaluation method, we claim this to be the remnant of Australia’s oldest yet known conventional oil accumulation at ~1.25 Ga. Analogous bituminous paleo-reservoirs from the North China Craton, dated at 1327 ± 2 Ma, were likely sourced from similar oil-prone cyanobacterial shales that formed during their shared connection with the North Australian Craton on the ancient supercontinent Nuna during the Mesoproterozoic.

Keywords: Beetaloo Sub-basin, burial history, fluid inclusions, GOI, McArthur Basin, Mesoproterozoic, Moroak Sandstone, North Australian Craton, North China Craton, Nuna, oil, petroleum supersystems, Roper Group, solid bitumen, Velkerri Formation.

Biographies

EP23047_B1.gif

Richard Kempton holds a BSc (Hons) in Geology from the University of Melbourne and a PhD from the University of Western Australia. Richard is a Senior Research Scientist with the Geofluids Team at CSIRO Energy in Perth and is a domain expert in fluid inclusions with 20+ years’ experience in reconstructing charge histories for petroleum systems analysis. More recently, he has been working on CO2 and hydrogen-related projects and geological applications of machine learning. Prior to joining CSIRO, Richard worked for the Queensland Gas Company. He is a member of PESA and the Geological Society of Australia.

EP23047_B2.gif

Siyumini Perera recently obtained her PhD from the University of Queensland, where she focussed on Early Paleozoic biostratigraphy and imaging of microfossils using micro-computed tomography. Since early 2023, she has joined the Geofluids Team at CSIRO Energy in Perth as a Research Technician and conducts various analyses to quantify and characterise geofluids within sedimentary basins and basement.

EP23047_B3.gif

Mohinudeen Faiz is a Geoscientist with 30+ years’ experience in petroleum exploration, development and research activities. Faiz holds PhD and MSc degrees from the University of Wollongong (Australia) and a BSc (Hons) degree from the University of Peradeniya (Sri Lanka). He is currently a Principal Research Scientist at CSIRO Energy where he focuses on basin modelling for petroleum systems and low-emission natural energy sources. Previously, Faiz worked at Origin Energy where he was an organic geochemistry and petroleum systems modelling subject matter expert and contributed to both conventional and unconventional exploration and production projects in various basins in Australia and overseas. He is a member of the American Association of Petroleum Geologists, PESA and International Committee for Coal and Organic Petrology.

EP23047_B4.gif

Michael Verrall is a Senior Research Scientist at CSIRO and is the Manager of the Electron Beam and X-ray Laboratories at the Australian Resource Research Centre. His interests are in scientific instrumentation and developing scanning electron microscopy and X-ray based techniques for automated mineralogy. Michael has a BSc degree in physics and previous experience working in the mining industry and also works as a Radiation Safety Officer for CSIRO.

References

Ahmad M, Dunster JN, Munson TJ (2013) ‘Chapter 15: McArthur Basin. In ‘Geology and mineral resources of the Northern Territory’. (Eds M Ahmad, TJ Munson). Special Publication 5. pp. 1–72. (Northern Territory Geological Survey)

Altmann C, Richards B, Côté A, Bein C, Baruch-Jurado E, Jenkinson L (2020) The Hayfield Sandstone Play: the characterisation of a Mesoproterozoic sourced, Proterozoic sandstone reservoirs, tight oil and gas play in the Beetaloo Sub-basin. The APPEA Journal 60, 242-266.
| Crossref | Google Scholar |

Bois C, Bouche P, Pelet R (1982) Global geologic history and distribution of hydrocarbon reserves. AAPG Bulletin 66, 1248-1270.
| Google Scholar |

Bourdet J, Eadington P, Volk H, George SC, Pironon J, Kempton R (2012) Chemical changes of fluid inclusion oil trapped during the evolution of an oil reservoir: Jabiru-1A case study (Timor Sea, Australia). Marine and Petroleum Geology 36, 118-139.
| Crossref | Google Scholar |

Bradshaw MT (1993) Australian petroleum systems. The PESA Journal 21, 43-53.
| Google Scholar |

Buick R, Rasmussen B, Krapez B (1998) Archean oil: evidence for extensive hydrocarbon generation and migration 2.5–3.5 Ga. AAPG Bulletin 82, 50-69.
| Google Scholar |

Camacho A, Armstrong R, Davis DW, Bekker A (2015) Early history of the Amadeus Basin: Implications for the existence and geometry of the Centralian Superbasin. Precambrian Research 259, 232-242.
| Crossref | Google Scholar |

Close DF (2014) The McArthur Basin: NTGS approach to a frontier petroleum basin with known base metal prospectivity. In ‘Proceedings of the Annual Geoscience Exploration Seminar (AGES), Alice Springs, Northern Territory, March 2014’. Record of Abstracts. Record 2014-001. pp. 85–89. (Northern Territory Geological Survey)

Close D, Côté A, Baruch E, Altmann C, Mohinudeen F, Richards B, Ilett R, Evans R, Stonier S (2017) Exploring the Beetaloo: will Australia’s first viable shale play be sourced by billion year old gas? The APPEA Journal 57, 716-721.
| Crossref | Google Scholar |

Côté A, Richards B, Altmann C, Baruch E, Close D (2018) Australia’s premier shale basin: five plays, 1,000,000,000 years in the making. The APPEA Journal 58, 799-804.
| Crossref | Google Scholar |

Cox GM, Jarrett A, Edwards D, Crockford PW, Halverson GP, Collins AS, Poirier A, Li Z-X (2016) Basin redox and primary productivity within the Mesoproterozoic Roper Seaway. Chemical Geology 440, 101-114.
| Crossref | Google Scholar |

Cox GM, Collins AS, Jarrett AJM, Blades ML, Shannon AV, Yang B, Farkas J, Hall PA, O’Hara B, Close D, Baruch ET (2022) A very unconventional hydrocarbon play: The Mesoproterozoic Velkerri Formation of northern Australia. AAPG Bulletin 106, 1213-1237.
| Crossref | Google Scholar |

Curiale JA (1986) Origin of solid bitumens, with emphasis on biological marker results. Organic Geochemistry 10, 559-580.
| Crossref | Google Scholar |

DeZotti A (2016) The supercontinent Columbia 1,590 million years ago. Available at https://commons.wikimedia.org/wiki/File:Paleoglobe_NO_1590_mya-vector-colors.svg

Duddy IR (2015) Jamison-1 well and ZK4001 borehole Beetaloo Sub-basin, Northern Territory. Reconstruction of thermal, burial and source rock maturation histories based on AFTA and organic reflectance data. Geotrack International Pty Ltd. Geotrack Report No. 1171. (Report prepared for Origin Energy: Brisbane)

Duddy IR, Green PF, Gibson J, Hegarty KA (2003) Regional palaeo-thermal episodes in northern Australia. In ‘Proceedings of the Timor Sea Symposium, Darwin, 19-20 June 2003’. (Eds PW Baillie, TJ Munson). pp. 567–591. (Northern Territory Geological Survey: Darwin)

Dutkiewicz A, Volk H, Ridley J, George SC (2007) Precambrian inclusion oils in the Roper Group: A review. In ‘Proceedings of the Central Australian basins symposium’. (Ed. TJ Munson, GJ Ambrose) pp. 326–348. (Northern Territory Geological Survey)

Eadington PJ, Lisk M, Krieger FW (1996a) Identifying oil well sites. Patent No. 5,543,616, United States

Eadington PJ, Lisk M, Krieger FW (1996b) Identifying oil well sites (Patent No. AU710401B2). Australia.

Evans DAD, Mitchell RN (2011) Assembly and breakup of the core of Paleoproterozoic–Mesoproterozoic supercontinent Nuna. Geology 39, 443-446.
| Crossref | Google Scholar |

Faiz M, Altmann C, Baruch E, Côté A, Gong S, Schinteie R, Ranasinghe P (2022) Organic matter composition and thermal maturity evaluation of Mesoproterozoic source rocks in the Beetaloo Sub-Basin, Australia. Organic Geochemistry 174, 104513.
| Crossref | Google Scholar |

Faiz M, Crombez V, Claudio DP, Lupton N, Camilleri M, Langhi L (2021) Petroleum systems model for source-rock-reservoir evaluation in the Beetaloo Sub-basin. In ‘Proceedings of the AEGC 2021 - Australasian Exploration Geoscience Conference, virtual online’. p. 6 (Australian Society of Exploration Geophysicists)

Goldstein RH, Reynolds TJ (1994) Chapter 1: Introduction to Fluid Inclusions and their Applications. In ‘Systematics of Fluid Inclusions in Diagenetic Minerals’. SEPM Short Course 31. pp. 1–3. (SEPM Society for Sedimentary Geology)

Gürsan C, de Gooyert V (2021) The systemic impact of a transition fuel: Does natural gas help or hinder the energy transition? Renewable and Sustainable Energy Reviews 138, 110552.
| Crossref | Google Scholar |

Han S, Lӧhr SC, Abbott AN, Baldermann A, Voigt M, Yu B (2022) Authigenic clay mineral evidence for restricted, evaporitic conditions during the emergence of the Ediacaran Doushantuo Biota. Nature Communications Earth & Environment 3, 165.
| Google Scholar |

Harwood J, Aplin AC, Fialips CI, Iliffe JE, Kozdon R, Ushikubo T, Valley JW (2013) Quartz cementation history of sandstones revealed by high-resolution SIMS oxygen isotope analysis. Journal of Sedimentary Research 83, 522-530.
| Crossref | Google Scholar |

Hoffman TW (2016) Roper Basin burial history modelling: Inferences for the timing of hydrocarbon generation. In ‘Proceedings of Northern Territory Geological Survey Annual Geoscience Exploration Seminar, Alice Springs, 15–16 March 2016’. pp. 107–117. (Northern Territory Geological Survey)

Jackson MJ, Southgate PN, Page RW (2000). Gamma-ray logs and U–Pb zircon geochronology essential tools to constrain lithofacies interpretation of Palaeoproterozoic depositional systems. In ‘Carbonate Sedimentation and Diagenesis in the Evolving Precambrian World’. (Eds JP Grotzinger, NP James). Special Publication 67. pp. 23–41. (SEPM Society for Sedimentary Geology)

Jarrett A, Edward D, Boreham C, McKirdy D (2016) Petroleum geochemistry of the Amadeus Basin. In ‘Annual Geoscience Exploration Seminar (AGES) Proceedings, Alice Springs, Northern Territory 15-16 March 2016’. Special Publication 67. pp. 37–42. (Northern Territory Geological Survey)

Jarrett AJM, Munson TJ, Williams B, Bailey AHE, Palu T (2022) Petroleum supersystems in the greater McArthur Basin, Northern Territory, Australia: prospectivity of the world’s oldest stacked systems with emphasis on the McArthur Supersystem. The APPEA Journal 62, 245-262.
| Crossref | Google Scholar |

Kendall B, Creaser RA, Gordon GW, Anbar AD (2009) Re–Os and Mo isotope systematics of black shales from the Middle Proterozoic Velkerri and Wollogorang formations, McArthur Basin, northern Australia. Geochimica et Cosmochimica Acta 73, 2534-2558.
| Crossref | Google Scholar |

Lander RH, Walderhaug O (1999) Predicting Porosity through Simulating Sandstone Compaction and Quartz Cementation. AAPG Bulletin 83, 433-449.
| Crossref | Google Scholar |

Lanigan KP (1992) Well completion report, EP33 – Elliott-1, Beetaloo Sub-basin of the McArthur Basin. Pacific Oil & Gas Limited. Northern Territory Geological Survey, Petroleum Report PR1992-0012

Lanigan K, Hibbird S, Menpes S, Torkington J (1994) Petroleum exploration in the Proterozoic Beetaloo Sub‑basin, Northern Territory. The APPEA Journal 34, 674-691.
| Crossref | Google Scholar |

Lavering LH, Passmore VL, Paton IM (1986) Discovery and exploitation of new oilfields in the Cooper-Eromanga basins. The APPEA Journal 26, 250-259.
| Crossref | Google Scholar |

Lessovaia SN, Polekhovsky YS (2009) Mineralogical composition of shallow soils on basic and ultrabasic rocks of East Fennoscandia and of the Ural Mountains, Russia. Clays and Clay Minerals 57, 476-485.
| Crossref | Google Scholar |

Lisk M, O’Brien GW, Brincat MP (1997) Gas displacement: an important control on oil and gas distribution in the Timor Sea. The APPEA Journal 37, 259-271.
| Crossref | Google Scholar |

Lisk M, O’Brien GW, Eadington PJ (2002) Quantitative evaluation of the oil-leg potential in the Oliver gas field, Timor Sea, Australia. AAPG Bulletin 86, 1531-1542.
| Google Scholar |

Liu Y, Zhong N, Tian Y, Qi W, Mu G (2011) The oldest oil accumulation in China: Meso-proterozoic Xiamaling Formation bituminous sandstone reservoirs. Petroleum Exploration and Development 38, 503-512.
| Crossref | Google Scholar |

Malek R, Mehin K (1998) ‘Oil and Gas Resources of Victoria.’ Special Publication. (Department of Natural Resources and Environment)

Marshall TR, Dyson IA, Liu K (2007) Petroleum systems in the Amadeus Basin, central Australia: Were they all oil prone? In ‘Central Australian Basins Symposium Proceedings, Alice Springs, August 2005’. (Eds TJ Munson, GJ Ambrose). Special Publication 2. pp. 136–146. (Northern Territory Geological Survey)

Meert JG, Santosh M (2017) The Columbia supercontinent revisited. Gondwana Research 50, 67-83.
| Crossref | Google Scholar |

Mohammad N, Ishak WWM, Mustapa SI, Ayodele BV (2021) Natural Gas as a Key Alternative Energy Source in Sustainable Renewable Energy Transition: A Mini Review. Frontiers in Energy Research 9,.
| Crossref | Google Scholar |

Mulder JA, Halpin JA, Daczko NR (2015) Mesoproterozoic Tasmania: Witness to the East Antarctica–Laurentia connection within Nuna. Geology 43, 759-762.
| Crossref | Google Scholar |

Munson TJ (2016) Sedimentary characterisation of the Wilton package, greater McArthur Basin, Northern Territory. Northern Territory Geological Survey (NTGS) Record 2016-003

Myers JS, Shaw RD, Tyler IM (1996) Tectonic evolution of Proterozoic Australia. Tectonics 15, 1431-1446.
| Crossref | Google Scholar |

Orr ML, Bernardel G, Owens R, Hall LS, Skeers N, Reese B, Woods M (2020) ‘Geology of the Beetaloo GBA region. Technical appendix for the Geological and Bioregional Assessment: Stage 2.’ (Department of the Environment and Energy, Bureau of Meteorology, CSIRO and Geoscience Australia, Australia)

Perera S, Kempton R, Wang H (2024) GOI/FOI™ sample analysis report – Balmain-1, Elliott-1, and Jamison-1. CSIRO Report EP2024-0337. (Submitted to the Northern Territory Geological Survey: Kensington, Australia)

Pesonen LJ, Mertanen S, Veikkolainen T (2012) Paleo-Mesoproterozoic supercontinents - A paleomagnetic view. Geophysica 48, 5-48.
| Google Scholar |

Pisarevsky SA, Elming SA, Pesonen LJ, Li Z-X (2014) Mesoproterozoic paleogeography: supercontinent and beyond. Precambrian Research 244, 207-25.
| Crossref | Google Scholar |

Purcell P, Longley I (2023) The North West Shelf, Western Australia’s super basin, in the twenty-first century. AAPG Bulletin 107, 1299-1367.
| Crossref | Google Scholar |

Rasmussen B (2005) Evidence for pervasive petroleum generation and migration in 3.2 and 2.63 Ga shales. Geology 33, 497-500.
| Crossref | Google Scholar |

Rawlings DJ (1999) Stratigraphic resolution of a multiphase intracratonic basin system: the McArthur Basin, northern Australia. Australian Journal of Earth Sciences 46, 703-723.
| Crossref | Google Scholar |

Sanei H (2020) Genesis of solid bitumen. Scientific Reports 10, 15595.
| Crossref | Google Scholar | PubMed |

Stasiuk LD, Snowdon LR (1997) Fluorescence micro-spectrometry of synthetic and natural hydrocarbon fluid inclusions: crude oil chemistry, density and application to petroleum migration. Applied Geochemistry 12, 229-241.
| Crossref | Google Scholar |

Towler BF (1986) Reservoir simulation in the Mereenie Field. The APPEA Journal 26, 428-446.
| Crossref | Google Scholar |

Volk H, Dutkiewicz A, George S, Ridley J (2003) Oil migration in the Middle Proterozoic Roper Superbasin, Australia: evidence from fluid inclusions and their geochemistries. Journal of Geochemical Exploration 78–79, 437-441.
| Crossref | Google Scholar |

Wang T (1991) Geochemical characteristics of the Longtangou bituminous sandstone in Lingyuan, eastern Yanshan region, north China–approach to a Precambrian reservoir bitumen. Journal of Southeast Asian Earth Sciences 5, 373-379.
| Crossref | Google Scholar |

Wang C, Li Z-X, Peng P, Pisarevsky S, Liu Y, Kirscher U, Nordsvan A (2019) Long-lived connection between the North China and North Australian cratons in supercontinent Nuna: paleomagnetic and geological constraints. Science Bulletin 64, 873-876.
| Crossref | Google Scholar | PubMed |

Wang X, Zhao W, Zhang S, Wang H, Su J, Canfield DE, Hammarlund EU (2018) The aerobic diagenesis of Mesoproterozoic organic matter. Scientific Reports 8, 13324.
| Crossref | Google Scholar |

Wang T-G, Zhong NN, Wang CJ, Zhu YX, Liu Y, Song DF (2016) Source beds and oil entrapment-alteration histories of fossil-oil-reservoirs in the Xiamaling Formation Basal Sandstone, Jibei Depression. Petroleum Science Bulletin 1, 24-37.
| Google Scholar |

Williams B (2019) Definition of the Beetaloo Sub‑basin. Record 2019-015. (Northern Territory Geological Survey (NTGS))

Yang B, Smith TM, Collins AS, Munson TJ, Schoemaker B, Nicholls D, Cox G, Farkas J, Glorie S (2018) Spatial and temporal variation in detrital zircon age provenance of the hydrocarbon-bearing upper Roper Group, Beetaloo Sub-basin, Northern Territory, Australia. Precambrian Research 304, 140-155.
| Crossref | Google Scholar |

Zhang S, Li Z-X, Evans DAD, Wu H, Li H, Dong J (2012) Pre-Rodinia supercontinent Nuna shaping up: A global synthesis with new paleomagnetic results from North China. Earth and Planetary Science Letters 353–354, 145-155.
| Crossref | Google Scholar |

Zhang S-H, Zhao Y, Li X-H, Ernst RE, Yang Z-Y (2017) The 1.33–1.30 Ga Yanliao large igneous province in the North China Craton: Implications for reconstruction of the Nuna (Columbia) supercontinent, and specifically with the North Australian Craton. Earth and Planetary Science Letters 465, 112-125.
| Crossref | Google Scholar |