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Australian Journal of Chemistry Australian Journal of Chemistry Society
An international journal for chemical science
RESEARCH ARTICLE (Open Access)

Development of a 3-D-printable device for continuous measuring of heavy metal ion concentrations

Charl de Villiers A , Magdalena Wajrak https://orcid.org/0000-0002-3666-2175 B * and Alex Lubansky C
+ Author Affiliations
- Author Affiliations

A Medi-Stats ANZ, 13 Mcrae Road, Sans Souci, NSW 2219, Australia.

B School of Science, Edith Cowan University, 270 Joondalup Drive, Joondalup, WA 6027, Australia.

C Haemograph Pty Ltd, 1/360 Ascot Vale Road, Moonee Ponds, Vic. 3039, Australia.

* Correspondence to: m.wajrak@ecu.edu.au

Handling Editor: Amir Karton

Australian Journal of Chemistry 76(12) 875-884 https://doi.org/10.1071/CH23112
Submitted: 14 June 2023  Accepted: 1 August 2023  Published online: 29 August 2023

© 2023 The Author(s) (or their employer(s)). Published by CSIRO Publishing. This is an open access article distributed under the Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International License (CC BY-NC-ND)

Abstract

Three-dimensional (3-D) printing offers the potential to create a range of tailored devices within many different industrial facilities. In this article, devices were designed and fabricated using 3-D printing to house electrodes for the testing of heavy metal concentration in hazardous fluids, particularly for biological samples such as urine or blood. The devices, connected to a syringe pump, were shown to be able to be operated without leaking. Proof of concept experiments were performed using Anodic Stripping Voltammetry (ASV) methods, demonstrating that the devices are able to be used for quick, cheap testing, showing the potential of the technique as a more hygienic analysis technique than conventional ASV with an immediacy that standard techniques such as inductively coupled plasma mass spectrometry (ICP-MS) do not offer. With further development and validation, 3-D-printed ASV techniques may provide a robust, reliable and affordable solution for heavy metal concentration detection in remote locations.

Keywords: 3-D-printed flow cell, electroanalytical chemistry, flow analysis, hazardous samples, lead, metal ions, microfluidic techniques, voltammetry.

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