Syntheses and Characterizations of Three Organically Templated Zinc Phosphites with 12-Ring Channels
Zhen-Zhen Bao A , Song-De Han A , Jin-Hua Li A , Guo-Ming Wang A B and Zong-Hua Wang A
+ Author Affiliations
- Author Affiliations
A College of Chemistry and Chemical Engineering, Collaborative Innovation Center for Marine Biomass Fiber Materials and Textiles, Qingdao University, Shandong 266071, China.
B Corresponding author. Email: gmwang_pub@163.com
Australian Journal of Chemistry 70(3) 286-292 https://doi.org/10.1071/CH16333
Submitted: 30 May 2016 Accepted: 15 August 2016 Published: 8 September 2016
Abstract
Three new zinc phosphites, [Hapy]2[Zn3(HPO3)4] (1; apy = 4-aminopyridine), [H2hepip][Zn3(HPO3)4]·(H2O)0.25 (2; hepip = N-(2-hydroxyethyl)piperazine), and [H2tmdab][Zn3(HPO3)4] (3; tmdab = N,N,N′,N′-tetramethyl-1,3-diaminobutane), have been synthesized and characterized by infrared spectroscopy, elemental analysis, thermogravimetric analysis, and powder and single-crystal X-ray diffraction. The frameworks of 1–3 are constructed from 4-connected ZnO4 tetrahedra and 3-connected HPO3 pseudo pyramids with distinct connection mode driven by different organic amine templates. There are 12-membered ring (12-MR) and 8-MR apertures in the (3,4)-connected three-dimensional architecture of 1–3. It is notable that helical chains are observed in the framework of compound 3.
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