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RESEARCH ARTICLE
Contents Vol 68(8)

Urothermal Syntheses, Crystal Structures, and Luminescent Properties of Two New ZnII Compounds Constructed by the Mixed Ligands of 1,2,4-Triazole and 1,4-Naphthalenedicarboxylic Acid or 2,6-Naphthalenedicarboxylic Acid

Haiyan Liu A , Xufeng Meng A , Lihui Zhang B and Anqiang Jia C D
+ Author Affiliations
- Author Affiliations

A College of Sciences, Agricultural University of Hebei, Baoding 071001, China.

B College of Plant Protection, Agricultural University of Hebei, Baoding 071001, China.

C Rural and Urban Construction College of Hebei Agricultural University, Baoding 071001, China.

D Corresponding author. Email: anqiang_jia3157@163.com

Australian Journal of Chemistry 68(8) 1299-1304 https://doi.org/10.1071/CH14669
Submitted: 21 November 2014  Accepted: 16 January 2015   Published: 26 March 2015

Abstract

Under urothermal conditions, the self-assembly of ZnII ions, 1,2,3-triazole, and two isomeric dicarboxylate ligands (1,4-H2ndc and 2,6-H2ndc) afforded two new metal–organic frameworks, namely [Zn(1,4-ndc)0.5(taz)]n·n(e-urea) (1) and [Zn(2,6-ndc)0.5(taz)]n·n(H2O)·n(e-urea) (2) (1,4-H2ndc = 1,4-naphthalenedicarboxylic acid; 2,6-H2ndc = 2,6-naphthalenedicarboxylic acid; Htaz = 1,2,4-triazole; e-urea = ethyleneurea), which were further determined by single-crystal X-ray diffraction analyses, elemental analyses, powder X-ray diffraction analyses, and IR spectra. Compound 1 features a 3D pillar-layered framework with 6-connected pcu topology (pcu = α-Po), and compound 2 also features a 3D pillar-layered framework with 6-connected pcu topology. In addition, the thermal stabilities and solid-state photoluminescent properties of compounds 1 and 2 were also studied.


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