
TY  - JOUR
A1  - Whyte, T 
A1  - Williams, GA 
T1  - Crystal Structure of Tetraethylammonium Bromopentacarbonyltungstate(0)
JF  - Australian Journal of Chemistry
JO  - Aust. J. Chem.
Y1  - 1995
VL  - 48
IS  - 5
SP  - 1045
EP  - 1048
KW  - 
UR  - https://doi.org/10.1071/CH9951045 
N2  - The crystal structure of tetraethylammonium  bromopentacarbonyltungstate (0), [NEt4] [W(CO)5Br], has been determined by single-crystal X-ray diffraction methods at 22±1&#176;C. Crystals are tetragonal, space group P4/n, with a 9.206(2), c 10.484(2) &#506;, and Z 2. Full-matrix least-squares refinement gave a final R value of 0.034 for 820 independent reflections. The [W(CO)5Br]- anion possesses exact C4v symmetry, with bond lengths W-Br 2.736(1), W-COtrans 1.93(1) and W-COcis 2.034(6) &#506;. 
ER  -

