
%0 Journal Article
%A Whyte, T 
%A Williams, GA 
%T Crystal Structure of Tetraethylammonium Bromopentacarbonyltungstate(0)
%J Australian Journal of Chemistry
%D 1995/05/01
%V 48
%N 5
%P 1045-1048
%K 
%R https://doi.org/10.1071/CH9951045
%U https://www.publish.csiro.au/paper/CH9951045 
%X The crystal structure of tetraethylammonium  bromopentacarbonyltungstate (0), [NEt4] [W(CO)5Br], has been determined by single-crystal X-ray diffraction methods at 22±1&#176;C. Crystals are tetragonal, space group P4/n, with a 9.206(2), c 10.484(2) &#506;, and Z 2. Full-matrix least-squares refinement gave a final R value of 0.034 for 820 independent reflections. The [W(CO)5Br]- anion possesses exact C4v symmetry, with bond lengths W-Br 2.736(1), W-COtrans 1.93(1) and W-COcis 2.034(6) &#506;. 
