
TY  - JOUR
A1  - Collins, DJ 
A1  - Jones, ED 
T1  - Regioselective 2,3-Di-O-silylation of Methyl 6-Chloro-6-deoxy-&#945;-D-glucopyranoside
JF  - Australian Journal of Chemistry
JO  - Aust. J. Chem.
Y1  - 1994
VL  - 47
IS  - 7
SP  - 1419
EP  - 1421
KW  - 
UR  - https://doi.org/10.1071/CH9941419 
N2  - Reaction of methyl 6-chloro-6-deoxy-&#945;-D-glucopyranoside (1) with an excess of t- butyldimethyl-silyl chloride in dimethylformamide in the presence of imidazole gave 53% of the corresponding 2,3-di-O-t-butyldimethylsilyl ether (2); under similar conditions D-gluconic acid 1,5-lactone (3) afforded 83% of the 2,3,4,6-tetra-O-t-butyldimethylsilyl ether (4). 
ER  -

