
%0 Journal Article
%A Collins, DJ 
%A Jones, ED 
%T Regioselective 2,3-Di-O-silylation of Methyl 6-Chloro-6-deoxy-&#945;-D-glucopyranoside
%J Australian Journal of Chemistry
%D 1994/07/01
%V 47
%N 7
%P 1419-1421
%K 
%R https://doi.org/10.1071/CH9941419
%U https://www.publish.csiro.au/paper/CH9941419 
%X Reaction of methyl 6-chloro-6-deoxy-&#945;-D-glucopyranoside (1) with an excess of t- butyldimethyl-silyl chloride in dimethylformamide in the presence of imidazole gave 53% of the corresponding 2,3-di-O-t-butyldimethylsilyl ether (2); under similar conditions D-gluconic acid 1,5-lactone (3) afforded 83% of the 2,3,4,6-tetra-O-t-butyldimethylsilyl ether (4). 
