
%0 Journal Article
%A Judd, MC 
%A Hartshorn, MP 
%A Martyn, RJ 
%A Robinson, WT 
%A Wright, GJ 
%A Vannoort, RW 
%T The Formation of Monomeric and Dimeric Nitro Nitrates in the Reaction of Phenanthrene With Nitrogen Dioxide: X-Ray Crystal Structure of <I>trans</I>-10-Nitro-9,10-dihydrophenanthren-9-yl Nitrate
%J Australian Journal of Chemistry
%D 1990/01/01
%V 43
%N 1
%P 125-132
%K 
%R https://doi.org/10.1071/CH9900125
%U https://www.publish.csiro.au/paper/CH9900125 
%X Reaction of phenanthrene (1) with nitrogen dioxide in benzene solution gives the dimeric nitro nitrate (3), trans and cis nitro nitrates (7) and (8), and 9-nitro- (4), 3-nitro- (5) and 1-nitro-phenanthrene (6). The X-ray crystal structure of the trans nitro nitrate (7) is reported. The effect of the phenanthrene (1) concentration on product yields is reported. Gas-liquid chromatography results for the nitro nitrates (3) and (7) point to difficulties in using this technique for product analyses in reactions of phenanthrene (1) with nitrogen dioxide. 
