
TY  - JOUR
A1  - Brice, MD 
A1  - Penfold, BR 
A1  - Robinson, WT 
T1  - Crystal and molecular structure of 4&#945;-t-Butylcyclohexane-1&#946;,2&#946;-diol
JF  - Australian Journal of Chemistry
JO  - Aust. J. Chem.
Y1  - 1972
VL  - 25
IS  - 10
SP  - 2117
EP  - 2124
KW  - 
UR  - https://doi.org/10.1071/CH9722117 
N2  - The crystal and molecular structure of 4&#945;-t-butylcyclohexane-1&#946;,2,&#946;-diol, C10H20O2, has been determined by X-ray diffraction methods. The compound crystallizes in the triclinic space group Pi with 4 molecules in a unit cell of dimensions a = 12.268, b = 15.921, c = 6.322Å, &#945; = 82.53, &#946; = 114.45, &#947; = 111.13°. The intensity data were measured by counter methods using Cu K&#945; radiation; the structure was solved by means of the tangent formula, and was refined using full matrix least-squares techniques to a final R-factor of 0.063 for 1199 reflections. The crystal structure consists of two sets of crystallographically non-equivalent molecules hydrogen-bonded to form discrete chains parallel to the c axis. The cyclohexane rings are in the chair conformation. 
ER  -

