The Crystal Structure of Tetraisothiocyanato-tetrakis(trimethylphosphine oxide)uranium(IV)
CEF Rickard and DC Woollard
Australian Journal of Chemistry
32(10) 2181 - 2185
Published: 1979
Abstract
The structure of the title compound has been determined by single-crystal X-ray crystallography. The crystals are orthorhombic, a 12·122(1), b 12·545(2), c 22·128(3) Å, space group Pccn. The structure was refined to a final residual of 0·040,1565 structure amplitudes being used. The molecules are eight-coordinate, the coordination polyhedron being an almost regular square antiprism, with the thiocyanate groups bonded through nitrogen.
https://doi.org/10.1071/CH9792181
© CSIRO 1979