Simple and Practical Synthesis of Various New Nickel Boride-Based Nanocomposites and their Applications for the Green and Expeditious Reduction of Nitroarenes to Arylamines under Wet-Solvent-Free Mechanochemical Grinding
Hossein Mousavi
A B , Behzad Zeynizadeh A , Reza Younesi A and Mozhgan Esmati A
+ Author Affiliations
- Author Affiliations
A Department of Organic Chemistry, Faculty of Chemistry, Urmia University, Urmia, Iran.
B Corresponding author. Email: 1hossein.mousavi@gmail.com
Australian Journal of Chemistry 71(8) 595-609 https://doi.org/10.1071/CH18200
Submitted: 2 May 2018 Accepted: 25 July 2018 Published: 22 August 2018
Abstract
In this paper, we report a simple synthesis of four new nickel boride-based nanocomposites, namely Ni2B@ZrCl4, Ni2B@Cu2O, Ni2B@CuCl2 and Ni2B@FeCl3, from commercially available and cheap starting materials. All of the new Ni2B-based nanocomposites were well characterized by Fourier-transform infrared spectroscopy, X-ray diffraction, scanning electron microscopy, and energy-dispersive X-ray spectroscopy. Further, the catalytic applications of these new nanocomposites were successfully evaluated in the wet-solvent-free reduction of aromatic nitro compounds to arylamines with sodium borohydride (NaBH4) at room temperature by a mechanochemical grinding technique. All the introduced catalytic systems provide excellent yields of arylamines in very short reaction times for a wide range of substrates. Also, recoverability and reusability of the new nanocomposites were investigated.
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