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Australian Journal of Chemistry Australian Journal of Chemistry Society
An international journal for chemical science
RESEARCH ARTICLE

The Synthesis and X-Ray Crystal Structure of t-Butyldimethylsilyl 2-[4-{4-(Hex-5-enyloxy)-phenylazo} phenyl]ethyl Ether

Daniel E. Lynch, Michael G. Forkan, L. Sid Miller and Simon Parsons

Australian Journal of Chemistry 51(11) 1053 - 1056
Published: 1998

Abstract

t-Butyldimethylsilyl 2-[4-{4-(hex-5-enyloxy)phenylazo}phenyl]ethyl ether (1) was synthesized on route to a polysiloxane system with azobenzene pendent groups. Compound (1) produced clear, orange-coloured crystals (space group P -1 with aa6·346(2), b 7·602(2),c 28·706(8) Å, α 89·84(2), β 85·17(2), γ 72· 29(2)°, Z 2) which allowed the structure to be determined by X-ray diffraction.

https://doi.org/10.1071/C98030

© CSIRO 1998

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