Lewis-Base Adducts of Lead(II) Compounds. II. Nine-Coordinate Capped Square-Antiprism Stereochemistry, [M(bidentate)4(unidentate)], in Tetrakis(1,10-phenanthroline)(perchlorato-O)lead(II) Perchlorate
LM Engelhardt, DL Kepert, JM Patrick and AH White
Australian Journal of Chemistry
42(2) 329 - 334
Published: 1989
Abstract
Improved precision, consequent upon redetermination of the structure of the title compound [Pb( phen )4(OCIO3)] (CIO4) [5184 'observed', 1 > 2 σ(I), diffractometer reflections; R 0.05 11, enables improved characterization of the nine-coordinate lead(II) environment in terms of a capped square antiprism.
https://doi.org/10.1071/CH9890329
© CSIRO 1989