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Australian Journal of Chemistry Australian Journal of Chemistry Society
An international journal for chemical science
RESEARCH ARTICLE

Crystal structure of Tris(ethane-1,2-diamine)nickel(II) diperchlorate monohydrate

CL Raston, AH White and AC Willis

Australian Journal of Chemistry 31(2) 415 - 418
Published: 1978

Abstract

The crystal structure of the title compound, [Ni(en)3] (ClO4)2,H2O, has been determined from single-crystal X-ray diffraction data at 295(1) K and refined by least squares to a residual of 0.093 for 1400 'observed' reflections. Crystals are orthorhombic, P bca, a 17.043(7), b 15.922(6), c 13.496(5) Ǻ, Z 8. The precision of the structure determination is adversely affected by very high perchlorate thermal motion. <Ni-N> is 2.13 Ǻ.

https://doi.org/10.1071/CH9780415

© CSIRO 1978

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