Crystal structure of exo-6-Bromo-exo-tricyclo[3,2,1,0^2,4]oct-anti-8-yl p-Nitrobenzoate

Abstract

The crystal structure of the title compound has been determined by single-crystal X-ray diffraction at 295 K and refined by least squares to a residual of 0.064 for 775 ?observed? reflections. The structure determination confirms the stereochemistry previously proposed for the molecule. Crystals are monoclinic, P2₁/n, a 11.131(7), b 18.908(3), c 7.121(5) Ǻ, β 104.56(5)°, Z 4.