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RESEARCH ARTICLE
Contents Vol 67(4)

Two NiII Complexes with Interesting Topologies Constructed from 5-Aminoisophthalic Acid with Rigid Bis(imidazole) Ligands

Fang-Hua Zhao A , Xin Zheng A B and Yun-Xia Che A C
+ Author Affiliations
- Author Affiliations

A Department of Chemistry, Nankai University, Tianjin, 300071, China.

B Department of Chemistry and Chemical Biology, and Department of Pharmaceutical Chemistry, Rutgers The State University of New Jersey, Piscataway, NJ 08854, USA.

C Corresponding author. Email: cheyx@nankai.edu.cn

Australian Journal of Chemistry 67(4) 603-608 https://doi.org/10.1071/CH13431
Submitted: 20 August 2013  Accepted: 16 October 2013   Published: 6 November 2013

Abstract

Two new NiII complexes, [Ni2(AIP)2(bib)1.5]·4H2O (1) and [Ni(AIP)(bibp)(H2O)]·H2O (2) (AIP = 5-aminoisophthalic acid, bib = 1,4-bis(1-imidazolyl)benzene and bibp = 4,4′-bis(1-imidazolyl)biphenyl), have been synthesised hydrothermally and characterised by IR, elemental, single-crystal X-ray diffraction, and powder X-ray diffraction analyses. Topology analysis reveals that complex 1 is a 2D bilayer network, containing a new tetranodal (3,3,4,5)-connected (63)2(65·8)(68·82) configuration. Complex 2 exhibits a 2D→3D inclined polycatenate framework based on the 2D 44-sql net. In addition, the thermal stability of the two complexes was also studied.


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