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Contents Vol 65(8)

Living Radical Polymerization by the RAFT Process – A Third Update

Graeme Moad A B , Ezio Rizzardo A and San H. Thang A
+ Author Affiliations
- Author Affiliations

A CSIRO Materials Science and Engineering, Bag 10, Clayton South, Vic. 3169, Australia.

B Corresponding author. Email: graeme.moad@csiro.au




Graeme Moad obtained his B.Sc. (Hons, First Class) and Ph.D. in organic free radical chemistry from Adelaide University. He joined CSIRO in 1979 and is currently a chief research scientist. Dr Moad is author/co-author of over 150 publications, co-inventor of 33 patent families and co-author of the book The Chemistry of Radical Polymerization. His research interests lie in the fields of polymer design and synthesis. In recognition of his work, Dr Moad was recently awarded the RACI’s Battaerd-Jordan Polymer Medal. Dr Moad is a titular member of the IUPAC Polymer Division and a Fellow of the RACI and the Australian Academy of Science.


Ezio Rizzardo FRACI, FTSE, FAA, FRS received his Ph.D. from the University of Sydney in 1969 and joined CSIRO in 1976 after post-doctoral research at Rice University, RIMAC, and the Australian National University. His CSIRO research has focused on developing methods for controlling free radical polymerization. He is co-author of some 200 journal papers with over 14,000 citations, and co-inventor on 44 worldwide patents. He has received a number of awards including the RACI Australian Polymer Medal, the CSIRO Chairman’s Gold Medal and an Australian Government Centenary Medal. In 2011, he was the co-recipient of the Prime Minister’s Prize for Science.


San H. Thang completed his Ph.D. in chemistry at Griffith University in 1987. Currently, he is a chief research scientist at CSIRO Materials Science and Engineering, and an adjunct professor at Monash University. San’s research focuses on the interface between biology and polymer chemistry. He has published over 100 papers which have to date received over 10,000 citations. He is responsible for several key inventions in the area of controlled/living radical polymerization; significantly, he is a co-inventor of the RAFT process. San is a Fellow of the Australian Academy of Technological Science and Engineering, and a Fellow of the Royal Australian Chemical Institute.

Australian Journal of Chemistry 65(8) 985-1076 https://doi.org/10.1071/CH12295
Submitted: 19 June 2012  Accepted: 25 July 2012   Published: 7 September 2012

Abstract

This paper provides a third update to the review of reversible deactivation radical polymerization (RDRP) achieved with thiocarbonylthio compounds (ZC(=S)SR) by a mechanism of reversible addition-fragmentation chain transfer (RAFT) that was published in June 2005 (Aust. J. Chem. 2005, 58, 379). The first update was published in November 2006 (Aust. J. Chem. 2006, 59, 669) and the second in December 2009 (Aust. J. Chem. 2009, 62, 1402). This review cites over 700 publications that appeared during the period mid 2009 to early 2012 covering various aspects of RAFT polymerization which include reagent synthesis and properties, kinetics and mechanism of polymerization, novel polymer syntheses, and a diverse range of applications. This period has witnessed further significant developments, particularly in the areas of novel RAFT agents, techniques for end-group transformation, the production of micro/nanoparticles and modified surfaces, and biopolymer conjugates both for therapeutic and diagnostic applications.


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