Group Position-Dependent Structurally Diverse Coordination Compounds Based on Isomeric Ligands
Jian Hua Zou A , Jian Nan Zhu A , Han Jie Cui A , Zhong Wang A , Da Liang Zhu A , He Tian A , Fei Fei Zhang A , Jing Wang A , Qiao Yun Li A B and Gao Wen Yang A B
+ Author Affiliations
- Author Affiliations
A Department of Chemistry and Material Engineering, Jiangsu Laboratory of Advanced Functional Materials, Changshu Institute of Technology, Changshu, 215500, China.
B Corresponding authors. Emails: liqiaoyun61@126.com; ygwsx@126.com
Australian Journal of Chemistry 68(6) 889-895 https://doi.org/10.1071/CH14442
Submitted: 1 April 2014 Accepted: 26 August 2014 Published: 18 November 2014
Abstract
Two isomeric ligands Htzpya and Hpytza (Htzpya = 3-(5-tetrazolyl)pyridine-1-acetic acid, Hpytza = 5-(3-pyridyl)tetrazole-2-acetic acid) have been selected to react with DyCl3·6H2O or PrCl3·6H2O under hydrothermal conditions, resulting in the formation of four new coordination compounds, mononuclear [Dy(tzpya)2(H2O)5]Cl·4H2O (1), dinuclear [Pr2(tzpya)2(H2O)12]Cl4·2H2O (2), and two one-dimensional polymers [Dy(pytza)2Cl(H2O)2]n (3) and [Pr(pytza)2Cl(H2O)2]n (4), whose structures are controlled by the different positions of the carboxylate group. These compounds were characterized by elemental analysis, infrared spectroscopy, thermogravimetric analysis, and single-crystal X-ray diffraction. Compounds 1–4 are self-assembled to form three-dimensional network structures by hydrogen bonding interactions. Furthermore, the luminescence properties were also investigated at room temperature in the solid state.
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